SamplePreparationSamplingandsamplepreparationisanimportantissuebecausetraditionalmethodsusedtoobtainsamplesforoxygenandnitrogendeterminationaredifferentfromthoserecommendedforhydrogen,especiallywhensamplingmoltenmetal.Themaindifferenceinsteelsamplingproceduresforoxygen/nitrogenandhydrogenisduetothemobilityofhydrogen.Specialprecautionsmustbeusedwhensamplingforhydrogen.Frommoltensteelandiron,asamplemustbequicklyquenchedincoldwaterandchilledinarefrigerantsuchasliquefiednitrogenoramixtureofacetoneandsolidcarbondioxideinordertoreducelossesofhydrogenfromdiffusion.Lossesofoxygenandnitrogenfromdiffusionarenotaproblem.Asamplethatistakenforhydrogenandchilledinarefrigerantcanalsobeusedforoxygenandnitrogendetermination.However,asamplethatistypicallytakenforoxygenand/ornitrogendeterminationisnotsuitableforhydrogendeterminationduetohydrogenloss(diffusion).Surfacecontaminationmustberemovedbyfilingorlightgrinding,usingcarenottooverheatthesample.分析儀,就選上海禹重實(shí)業(yè)有限公司,用戶的信賴之選。安徽專業(yè)元素分析儀咨詢報(bào)價(jià)
Instrumentcalibration/driftcorrectionf.Cleantheupperandlowerelectrodemanually,or,ifapplicable,removethecrucibleandpresstheanalyzebuttontocleanwiththeautomaticcleaner.g.Firmlyplaceagraphitecrucibleonthelowerelectrodetip.h.PresstheAnalyzebuttonontheinstrumentscreen,thelowerelectrodewillcloseandtheanalysissequencewillstartandendautomatically.i.Repeatsteps3bthrough3haminimumofthreetimesforeachcalibration/driftstandardused..Calibrate/driftfollowingtheprocedureoutlinedintheoperatorsinstructionmanual.山東專業(yè)元素分析儀多少錢上海禹重實(shí)業(yè)有限公司分析儀服務(wù)值得放心。
Oxygen,Nitrogen,andHydrogeninRefractoryMetalsSummaryOxygenandnitrogenarealloyingelementsintitanium,andarealsoclassifiedasalphastabilizingelementsastheypromotealphaphasealloys.Interstitialoxygenandnitrogenlevelscanbeusedtoregulatethetensilestrengthofthematerial,butduetoitshighsolubilitycancauseunwantedsurfaceembrittlement.Thisphenomenoncanbeleveraged,however,undercontrolledprocessingtocreatesurfacefilmsthatincreasesurfacehardnessandwearproperties.
SummaryThedeterminationoftheamountofoxygen,nitrogen,andhydrogeniniron,steel,nickel-,andcobalt-basealloysrepresentssomeofthemostimportantqualitymetricsforthesematerials.Oxygenisusedtocreatesteelfrompigironbyremovingexcesscarbon.Oxygencontentmustbecontrolledtolimittheamountofcarbonmonoxidethatcanbeformedduringsolidificationwhichmaycauseexcessiveporosity.Nitrogenisconsideredbothanimpurityaswellasanimportantalloyingagent.Itcanbepresentasanitrideorinterstitiallyinitsgaseousform.Increasednitrogencontentisknowntoincreaseyieldandtensilestrength,thusdecreasingductilityandformability.Excessivelevelsmayevolveduringsolidificationthusincreasingporosity.Highhydrogencontentistheprimarycauseofembrittlement,blisteringandflakingduetoitshighmobilitythroughthelatticeandprovidesnopotentialalloyingbenefits.TheONH836utilizesahigh-powerelectrodefurnacetoquicklyandefficientlyreleasethetargetgasesfromwithinthesample,whichallowsforaveryrapidsimultaneousdeterminationofoxygen,nitrogen,andhydrogen.上海禹重實(shí)業(yè)有限公司是一家專業(yè)提供分析儀的公司,有想法的不要錯(cuò)過哦!
Procedure–Powder/ChipSamplesInstrumentcalibration/driftcorrection.PresstheAnalyzebuttonontheinstrumentscreen.Afterashortdelay,theloadingheadslide-blockwillopen.PlacetheNickelCapsulecontainingthesampleintotheopenportatthetopoftheloadinghead.PresstheAnalyzebuttonontheinstrumentscreenagain,theloadingheadslide-blockwillcloseandthelowerelectrodewillopen.Cleantheupperandlowerelectrodeeithermanuallyorremovethecrucibleandpresstheanalyzebuttontocleanwithanautomaticcleanerifapplicable.上海禹重實(shí)業(yè)有限公司為您提供分析儀,歡迎新老客戶來電!浙江美國LECO分析儀廠家供應(yīng)
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